ASTM A262 PRACTICE C PDF

Nitric Acid, ASTM A, Practice C, (Huey Test) The specimens are boiled for five periods, each of 48 hours, in a 65 per cent solution of nitric acid. The corrosion. employed to measure the relative susceptibility of austenitic stainless steels to intergranular attack. ASTM A Practice C, boiling nitric acid test is also known . Ferric Sulfate – Sulfuric Acid, ASTM A – Practice B (Stretcher Test). Ferric Sulfate Nitric Acid, ASTM A, Practice C, (Huey Test). Nitric Acid, ASTM A

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These tests do not provide a a26 for predicting resistance to forms of corrosion other than intergranular, such as general corrosion, pitting, or stress-corrosion cracking. The Strauss test is commonly used to evaluate the heat-treatment of as-received material, the effectiveness of alloying additions of elements such as Nb and Ti, or the effectiveness of reducing carbon content to resist intergranular attack.

Choosing the correct method s rely on a complete understanding of your material and processes, as well as the concept of corrosion itself.

The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. The Huey test works well to analyze chromium depleted regions and intermetallic precipitates, such as sigma phase, and is also used for materials in strongly astk environments such as nitric acid.

Due to the oractice of attack in different materials, numerous methods Practices B-F are used to assess intergranular corrosion.

However, when a622 material is exposed to high temperatures for long periods of time, a process called sensitization may occur. Please share this page: The first and fastest step is the ASTM A Practice A, a rapid same-day screening method in Oxalic acid to determine the susceptibility to intergranular corrosion. Each ASTM A Practice specification includes a list of the grades of stainless steels and the acceptable etch structures for the specific alloys.

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Please specify prsctice maximum allowable corrosion rate and any available data on the sensitizing heat treatment performed. It is typically used for stainless alloys such as andCr-Ni-Mo stainless alloys, and nickel alloys to evaluate the intergranular attack associated with the precipitation of chromium carbides at grain boundaries. In everyday applications, corrosion varies by materials and ;ractice.

ASTM A Intergranular Corrosion Testing and Analysis

In many cases we can reduce that to as little as 24 hours more than the required testing time if you need fast results. For example, in highly oxidizing solutions, intergranular attack can occur due to intermetallic phases, while attack of carbides may occur somewhat less oxidizing solutions. Some specific hazards statements are given in Choosing an Intergranular Corrosion Test Method Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.

This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively. The etch structure types used to classify the specimens are: The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack. For example, many low-carbon and stabilized stainless steels e. Since high temperature processing such as heat treatment is a common practice, many manufacturers wish to perform intergranular corrosion qualification testing on each batch, to ensure that the material has been processed correctly and does not show signs of corrosion susceptibility.

It depends on which Practice is selected, but typically ranges from to days for different tests.

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Intergranular Corrosion Testing: An Overview of ASTM A262

Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing praactice for your material while providing actionable results you can rely on. The weight loss is calculated after each step, and reveals if the sample has been properly heat-treated.

How do you select the right ASTM corrosion testing method for your material?

Because it can be run quickly for screening, we often run this test first. In SEM analysis, intergranular corrosion is clear by the dark lines where the grain boundaries are eaten away. Classification of the structure after A Practice A analysis will determine if the material is acceptable or if additional testing is required.

This abstract is a brief summary of the referenced standard.

Intergranular corrosion occurs as a result of precipitation of nitridescarbidesand other intermetallic phasessuch as sigma phase, that occurs along the grain boundaries. Historical Version s – view previous versions of standard. Contact us now for pricing or a quote! The test is generally performed for acceptance of materials, but practicd sufficient for rejection of materials.

The Oxalic Acid test is also only applicable to corrosion associated with chromium carbide precipitates and is only useful for specific material grades.

These practices include five intergranular corrosion tests, namely: Practice A, the oxalic acid etch test is used as a rapid technique to screen samples of certain stainless steel grades to ensure they are not susceptible to intergranular attack sensitization. Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular s262.